Organic Synthesis 7-D-SK.EN-06

Learning content
Form of classes Seminar (S)
W01 The theory of valence bonds and molecular orbitals. Types of chemical bonds. Molecules' electron density. Localized and delocalized covalent bond. The theory of resonance. The order of carbon atom.
W02 Basic structural elements of the carbon skeleton. Biological importance. Structure-activity relationship. Isomers and stereoisomers. Selected aspects of synthesis
W03, W04, W05 Review of functional groups of organic compounds. Occurrence in nature and economic importance. Examples of industrial production and laboratory synthesis.
W06, W07 Electronic databases of organic compounds.
Form of classes Laboratory (L)
L01, L02 Health and safety at work in the laboratory. Basic laboratory equipment. Installation of glass apparatus.
L03, L04 Distillation: • simple • fractional • steam • operation of a rotary evaporator. Determinants of the homogeneity of a chemical compound: • boiling point determination • refractive index.
L05 Crystallization: • temperature-controlled • solvent / anti-solvent • melting point determination.
L06 Extraction: • liquid / liquid • Soxhlet apparatus.
L07 Chromatography: • thin layer (TLC) • column chromatography.
L08-L15 Selected syntheses of organic compounds constituting an overview of the basic mechanisms of organic chemistry reactions. Reactions characteristic for individual functional groups.

Supplementary literature

1 http://www.bojensen.net/EssentialOilsEng/EssentialOils.htm 2 https://en.wikipedia.org/wiki/Category:World_Health_Organization_essential_medicines 3 http://www.chemspider.com/StructureSearch.aspx 4 https://www.nmrdb.org/

Student workload

Summary quantitative indicators ECTS The number of ECTS points obtained by a student during classes that require the direct participation of academic teachers (contact hours) 3,0 The number of ECTS points that a student obtains without the direct participation of an academic teacher (student's own work) 3,0 The number of ECTS points that the student obtains during theoretical classes (seminar) 1,2 The number of ECTS points that the student obtains during practical classes (laboratory) 4,8 Student workload Form of activity Number of hours ECTS Contact hours: theoretical practical theoretical practical participation in classes 15 60 0,6 2,4 credit Sum: 75 3,0 Student's own work: theoretical practical theoretical practical preparation for classes 5 50 0,6 2,4 preparation for passing 10 10 Sum: 75 3,0 Together: 150 6,0

Type of course

obligatory courses

Requirements

Basic organic chemistry course

Prerequisites

No. Learning objectives O1 Students are able to recognize the basic structural elements of organic compounds including stereochemistry O2 Students know the basics of the synthesis of organic compounds O3 Students practice laboratory techniques for the separation and purification of organic compounds O4 Students practice the synthesis of organic compounds

Learning outcomes

No. Learning outcomes (subject) Study field effects Area effects
Knowledge
K_01 presents the basic structural element of organic compounds, taking into account the stereochemistry P6S_WG
K_02 knows the basic rules of the nomenclature of organic compounds according to the IUPAC nomenclature P6S_WG
K_03 explains the theoretical basis of laboratory techniques for the separation and purification of organic compounds (in particular: distillation, extraction, crystallization, chromatography). P6S_WG
K_04 plans a method of synthesizing simple organic compounds P6S_WG
Skills
S_01 determines the relationship between the molecular structure of organic compounds and their chemical and physical properties P6S_UW, P6S_UK, P6S_UW
S_02 wykorzystuje podstawowe dane z widm NMR, IR, MS, UV-Vis do przedstawienia struktury prostych związków organicznych P6S_UW
P6S_UO
S_03 assembles laboratory kits to conduct one-step reactions P6S_UW, P6S_UO
S_04 uses basic laboratory equipment P6S_UW, P6S_UO
S_05 determines the homogeneity of an organic compound based on its physical data and thin layer chromatography P6S_UW, P6S_UO
S_06 isolates selected simple organic compounds from a reaction mixture or a natural source using basic laboratory techniques (in particular: filtration, distillation, extraction, crystallization, chromatography) P6S_UW
S_07 performs simple reactions for the synthesis of organic compounds with the use of basic glass and laboratory equipment P6S_UW, P6S_UO,
S_08 keep notes in a lab journal P6S_UW, P6S_UK
Social competences (attitudes)
C_01 understands the need for systematic education P6S_KR
P6S_KO
C_02 is aware of the responsibility for the safety of his own work and work in neighboring positions P6S_KO,
C_03 understands the need for systematic and reliable work while conducting organic synthesis P6S_KO
C_04 is aware of the dangers of using chemicals P6S_KO

Assessment criteria

No. Teaching methods
M1 didactic discussion
M2 database analysis
M3 laboratory exercises
M4 consultations (organized in individual cases),

Assessment methods
Formative assessment
It expresses the results that students obtained during the classes, carried out at the beginning and during the classes:
test / test
oral answer
laboratory exercise report
carrying out a practical exercise
activity in the classroom Summative assessment
Summarizes the achieved learning outcomes, carried out at the end of the class:
written exam / test
oral exam / test
test
final / semester work
multimedia presentation
report on field activities
weighted average of forming scores
FA1 activity in the classroom OP1 semester work
FA2 carrying out a practical exercise OP2 weighted average of forming scores

Additional information

Additional information (registration calendar, class conductors, localization and schedules of classes), might be available in the USOSweb system:

Description of 7-D-SK.EN-06 in USOSweb